| Good Samples Mean
Good Test Results
Soil Sampling
Procedures
Feed Sampling Procedures
Plant Sampling Procedures
Water Sampling Procedures
Liquid Fertilizer Sampling Procedures
Soil Sampling Procedures
1. Tools (Equipment) Use any of the tools shown
below, one or two clean pails and soil bags.

2. Sampling Depth
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- Surface soil samples from fields should be taken to a depth
of 8".
- Subsoil samples should be taken from 8" to 36"
for residual nitrate. An alternative method would be to sample 8-24" and 24-48".
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3. Sample each field separately
If cropping, fertilization and/or liming has not been
uniform on a field, then a separate sample should be taken from each management or soil
area. If fields are large, you may want to sample 40 acre units separately, but it is not
necessary if management has been the same and the soil type is the same. If soil areas
within a field are different in appearance (slope, drainage, color or texture), each soil
area should be sampled separately. Small areas may not need to be sampled, but they will
give some indication of the variation within the field.
4. Composite surface soil samples should consist of
a mixture of about 15 soil cores. Composite subsoil samples for the nitrate test should
consist of 8-10 cores. Mix these core thoroughly and fill the sample bag. Label the bag
correctly and use this same identification on the soil information sheet.
5. Sample separately or avoid such areas as dead
furrows, alkali spots and terrace channels.
6. Send samples as quickly as possible. Include
soil sample information sheets.
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Feed Sampling Procedures
Hay
- Bales: Sample at least 8 to 12 bales from each cutting or
each lot. Core all rectangular bales from the end and all round bales from the twine
surface. Mix the samples thoroughly and take a representative sample for analysis using
the quartering procedure.
- Loose Hay Stacks: Select 4 stacks from each cutting for
sampling. Collect at least 3 core samples from the side of each stack, mix thoroughly and
take a representative sample for analysis using the quartering
procedure. If a core sampler is not used for hay sampling, hand grab from each of
the bales.
Silage
Bunk sample
- Take 6-8 grab samples from the bunk(s) as the ration is
being unloaded. Mix the sample thoroughly and take a representative sample for analysis
using the quartering procedure.
Grain sample
- Take 5 random hand samples from the bin or truck. Mix the
sample thoroughly and take a representative sample for analysis using the quartering procedure.
Quartering Procedure:
- Sometimes when forages are sampled, the total of the
aggregate samples is to large and bulky to send in to the laboratory. The total sample
size can be properly reduced and still maintain a representative sample by quartering the
sample. Mix the entire sample thoroughly, then pour it into a pile on a clean paper or
plastic. Then divide the sample into four equal parts (quarters), saving the opposite two
quarters. If the sample is still to large, repeat the procedure until the proper sample
size of one pint to a quart is obtained. All samples should be placed in an airtight
plastic bag and submitted to the laboratory for analysis.
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Plant Sampling Procedures
| Field Crops |
Stage of Growth |
Plant Part to Sample |
# of Plants |
| Corn |
Seedling stage (less than 12")
Prior to tasseling
Tasseling to early silking |
All above ground portion
Top leaf with collar
Ear leaf |
20-30
15-25
15-25 |
| Soybeans |
Seedling stage (less than 12")
Initial flowering |
All above ground portion
Uppermost fully developed trifoliate leaves |
20-30
20-30 |
| Small grain |
Seedling stage (less than 12")
Boot to heading |
All above ground portion
All above ground portion |
50-100
20-30 |
| Hay, pasture or forage grasses |
Just prior to seed head emergence or 4 to 6 weeks after
clipping |
All above ground portion |
20-30 |
| Alfalfa |
Bud stage to 1/10 bloom |
Upper 1/3 of plant |
15-25 |
| Milo |
Very early heading |
2nd leaf from the top |
15-25 |
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Water Sampling Procedures
- Use a clean plastic container for submitting your sample.
Bottles can be obtained from the laboratory.
- Rinse the container several times with water that is being
sampled. Send at least one-half pint of water to be tested.
- Wells should be pumped several hours before sampling. Test
wells should be sampled after pipe and screen are in place. Pump well for at least 10
hours before sampling.
- Samples of lakes, streams, and ponds should be taken from
below surface.
- If it is not possible to send the sample to the lab
immediately after collection, refrigerate until it is sent.
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Liquid Fertilizer Sampling Procedures
A critical requirement in getting a representative sample
of a liquid fertilizer is to take the sample directly from the main body of the material
without contamination. Avoid, whenever possible, taking samples from lines and valves.
Listed below are the preferred points of sampling in order of preference.
- Directly from mixing vat.
- From the top opening of storage or transport tank after
agitating for 15 minutes.
- From a delivery or recirculating line after proper
recirculation.
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