Good Samples Mean Good Test Results

Soil Sampling Procedures
Feed Sampling Procedures
Plant Sampling Procedures
Water Sampling Procedures
Liquid Fertilizer Sampling Procedures

Soil Sampling Procedures

1. Tools (Equipment) Use any of the tools shown below, one or two clean pails and soil bags.

2. Sampling Depth

 
  • Surface soil samples from fields should be taken to a depth of 8".
  • Subsoil samples should be taken from 8" to 36" for residual nitrate. An alternative method would be to sample 8-24" and 24-48".

3. Sample each field separately

If cropping, fertilization and/or liming has not been uniform on a field, then a separate sample should be taken from each management or soil area. If fields are large, you may want to sample 40 acre units separately, but it is not necessary if management has been the same and the soil type is the same. If soil areas within a field are different in appearance (slope, drainage, color or texture), each soil area should be sampled separately. Small areas may not need to be sampled, but they will give some indication of the variation within the field.

4. Composite surface soil samples should consist of a mixture of about 15 soil cores. Composite subsoil samples for the nitrate test should consist of 8-10 cores. Mix these core thoroughly and fill the sample bag. Label the bag correctly and use this same identification on the soil information sheet.

5. Sample separately or avoid such areas as dead furrows, alkali spots and terrace channels.

6. Send samples as quickly as possible. Include soil sample information sheets.

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Feed Sampling Procedures

Hay

  • Bales: Sample at least 8 to 12 bales from each cutting or each lot. Core all rectangular bales from the end and all round bales from the twine surface. Mix the samples thoroughly and take a representative sample for analysis using the quartering procedure.

   

  • Loose Hay Stacks: Select 4 stacks from each cutting for sampling. Collect at least 3 core samples from the side of each stack, mix thoroughly and take a representative sample for analysis using the quartering procedure. If a core sampler is not used for hay sampling, hand grab from each of the bales.

     

Silage

  • Upright silo: Take random handfuls of silage while unloading. Mix the samples thoroughly and take a representative sample for analysis using the quartering procedure.

    Horizontal silo: Remove a column 6 inches by 12 inches wide on the open end of the silo. Mix the sample thoroughly and take a representative sample for analysis using the quartering procedure.

Bunk sample

  • Take 6-8 grab samples from the bunk(s) as the ration is being unloaded. Mix the sample thoroughly and take a representative sample for analysis using the quartering procedure.

Grain sample

  • Take 5 random hand samples from the bin or truck. Mix the sample thoroughly and take a representative sample for analysis using the quartering procedure.

Quartering Procedure:

  • Sometimes when forages are sampled, the total of the aggregate samples is to large and bulky to send in to the laboratory. The total sample size can be properly reduced and still maintain a representative sample by quartering the sample. Mix the entire sample thoroughly, then pour it into a pile on a clean paper or plastic. Then divide the sample into four equal parts (quarters), saving the opposite two quarters. If the sample is still to large, repeat the procedure until the proper sample size of one pint to a quart is obtained. All samples should be placed in an airtight plastic bag and submitted to the laboratory for analysis.

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Plant Sampling Procedures

Field Crops Stage of Growth Plant Part to Sample # of Plants
Corn Seedling stage (less than 12")
Prior to tasseling
Tasseling to early
silking
All above ground portion
Top leaf with collar
Ear leaf
20-30
15-25
15-25
Soybeans Seedling stage (less than 12")
Initial flowering
All above ground portion
Uppermost fully developed trifoliate leaves
20-30
20-30
Small grain Seedling stage (less than 12")
Boot to heading
All above ground portion
All above ground portion
50-100
20-30
Hay, pasture or forage grasses Just prior to seed head emergence or 4 to 6 weeks after clipping All above ground portion 20-30
Alfalfa Bud stage to 1/10 bloom Upper 1/3 of plant 15-25
Milo Very early heading 2nd leaf from the top 15-25

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Water Sampling Procedures

 

  1. Use a clean plastic container for submitting your sample. Bottles can be obtained from the laboratory.
  2. Rinse the container several times with water that is being sampled. Send at least one-half pint of water to be tested.
  3. Wells should be pumped several hours before sampling. Test wells should be sampled after pipe and screen are in place. Pump well for at least 10 hours before sampling.
  4. Samples of lakes, streams, and ponds should be taken from below surface.
  5. If it is not possible to send the sample to the lab immediately after collection, refrigerate until it is sent.

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Liquid Fertilizer Sampling Procedures

A critical requirement in getting a representative sample of a liquid fertilizer is to take the sample directly from the main body of the material without contamination. Avoid, whenever possible, taking samples from lines and valves. Listed below are the preferred points of sampling in order of preference.

 

  1. Directly from mixing vat.
  2. From the top opening of storage or transport tank after agitating for 15 minutes.
  3. From a delivery or recirculating line after proper recirculation.